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In this study, levulinic acid (LA) was produced from rice straw biomass in co-solvent biphasic reactor system consisting of hydrochloric acid and dichloromethane organic solvent. The modified protocol achieved a 15% wt LA yield through the synergistic effect of acid and acidic products (auto-catalysis) and the designed system allowed facile recovery of LA to the organic phase. Further purification of the resulting extractant was achieved through traditional column chromatography, which yielded a high purity LA product while recovering ∼85% wt. Upon charcoal treatment of the resultant fraction generated an industrial grade target molecule of ∼99% purity with ∼95% wt recovery. The system allows the solvent to be easily recovered, in excess of 90%, which was shown to be able to be recycled up to 5 runs without significant loss of final product concentrations. Overall, this system points to a method to significantly reduce manufacturing cost during large-scale LA preparation.

In this study, levulinic acid (LA) was produced from rice straw biomass in co-solvent biphasic reactor system consisting of hydrochloric acid and dichloromethane organic solvent. The modified protocol achieved a 15% wt LA yield through the synergistic effect of acid and acidic products (auto-catalysis) and the designed system allowed facile recovery of LA to the organic phase. Further purification of the resulting extractant was achieved through traditional column chromatography, which yielded a high purity LA product while recovering ∼85% wt. Upon charcoal treatment of the resultant fraction generated an industrial grade target molecule of ∼99% purity with ∼95% wt recovery. The system allows the solvent to be easily recovered, in excess of 90%, which was shown to be able to be recycled up to 5 runs without significant loss of final product concentrations. Overall, this system points to a method to significantly reduce manufacturing cost during large-scale LA preparation.

Abstract Newer generation sources and loads are posing new challenges to the conventional power system protection schemes. Adaptive and intelligent protection methodology, based on advanced measurement techniques and intelligent fault diagnosis such as machine learning (ML), is found to be useful to meet these challenges. A large number of research works are reported on ML-based power system fault diagnosis. However, ML techniques are evolving at a very fast pace, and an inclusive, as well as state-of-the-art review on ML-based power system fault diagnosis, is not available in the literature. Given this need and growing trend towards ML, the study presented in this paper aims to provide a comprehensive review of ML-based power system fault diagnosis. At first, efforts have been made to enlist the issues present in conventional fault diagnosis which led to the popularity of ML techniques. Also, a baseline framework and workflow for ML-based fault diagnosis are presented. Next, various unsupervised and supervised learning techniques have been discussed separately which have been used by several researchers for fault diagnosis. The discussion throughout is supported with tabulated facts for fault detection, classification and localization works with techniques used, different simulation tools used, and their application system. The advantages and disadvantages of all the techniques of fault diagnosis have also been discussed which will help the readers in the selection of techniques for their research. A brief review of reinforcement learning and transfer learning is also given as they are gaining popularity in power system-related studies and have the potential to be used for fault diagnosis. Finally, the research trends, some key issues, and directions for future research have been highlighted.

Abstract Newer generation sources and loads are posing new challenges to the conventional power system protection schemes. Adaptive and intelligent protection methodology, based on advanced measurement techniques and intelligent fault diagnosis such as machine learning (ML), is found to be useful to meet these challenges. A large number of research works are reported on ML-based power system fault diagnosis. However, ML techniques are evolving at a very fast pace, and an inclusive, as well as state-of-the-art review on ML-based power system fault diagnosis, is not available in the literature. Given this need and growing trend towards ML, the study presented in this paper aims to provide a comprehensive review of ML-based power system fault diagnosis. At first, efforts have been made to enlist the issues present in conventional fault diagnosis which led to the popularity of ML techniques. Also, a baseline framework and workflow for ML-based fault diagnosis are presented. Next, various unsupervised and supervised learning techniques have been discussed separately which have been used by several researchers for fault diagnosis. The discussion throughout is supported with tabulated facts for fault detection, classification and localization works with techniques used, different simulation tools used, and their application system. The advantages and disadvantages of all the techniques of fault diagnosis have also been discussed which will help the readers in the selection of techniques for their research. A brief review of reinforcement learning and transfer learning is also given as they are gaining popularity in power system-related studies and have the potential to be used for fault diagnosis. Finally, the research trends, some key issues, and directions for future research have been highlighted.

Microalgae are promising sources of valuable compounds: carotenoids, polyunsaturated fatty acids, lipids, etc. To overcome the feasibility challenge due to low yield and attain commercial potential, researchers merge technologies to enhance algal bioprocess. In this context, nanomaterials are attractive for enhancing microalgal bioprocessing, from cultivation to downstream extraction. Nanomaterials enhance biomass and product yields (mainly lipid and carotenoids) through improved nutrient uptake and stress tolerance during cultivation. They also provide mechanistic insights from recent studies. They also revolutionize harvesting via nano-induced sedimentation, flocculation, and flotation. Downstream processing benefits from nanomaterials, improving extraction and purification. Special attention is given to cost-effective extraction, showcasing nanomaterial integration, and providing a comparative account. The review also profiles nanomaterial types, including metallic nanoparticles, magnetic nanomaterials, carbon-based nanomaterials, silica nanoparticles, polymers, and functionalized nanomaterials. Challenges and future trends are discussed, emphasizing nanomaterials' role in advancing sustainable and efficient microalgal bioprocessing, unlocking their potential for bio-based industries.

Microalgae are promising sources of valuable compounds: carotenoids, polyunsaturated fatty acids, lipids, etc. To overcome the feasibility challenge due to low yield and attain commercial potential, researchers merge technologies to enhance algal bioprocess. In this context, nanomaterials are attractive for enhancing microalgal bioprocessing, from cultivation to downstream extraction. Nanomaterials enhance biomass and product yields (mainly lipid and carotenoids) through improved nutrient uptake and stress tolerance during cultivation. They also provide mechanistic insights from recent studies. They also revolutionize harvesting via nano-induced sedimentation, flocculation, and flotation. Downstream processing benefits from nanomaterials, improving extraction and purification. Special attention is given to cost-effective extraction, showcasing nanomaterial integration, and providing a comparative account. The review also profiles nanomaterial types, including metallic nanoparticles, magnetic nanomaterials, carbon-based nanomaterials, silica nanoparticles, polymers, and functionalized nanomaterials. Challenges and future trends are discussed, emphasizing nanomaterials' role in advancing sustainable and efficient microalgal bioprocessing, unlocking their potential for bio-based industries.