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Journal of the European Ceramic Society
Article . 2022 . Peer-reviewed
License: CC BY
Data sources: Crossref
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Development and comparison of field assisted sintering techniques to densify CeO2 ceramics

Authors: Harrison, Robert; Morgan, Jonathan; Buckley, James; Bostanchi, Samira; Green, C.; White, R.; Pearmain, D.; +3 Authors

Development and comparison of field assisted sintering techniques to densify CeO2 ceramics

Abstract

Cerium dioxide (CeO2) was densified by conventional and field assisted sintering techniques in order to examine the effect of a range of sintering parameters on the resultant pellet microstructure, namely: temperature, hold time, atmosphere, electric field strength and polarity. CS at 1400C for 2 hours in static air atmospheres provided the highest densities and grain sizes compared with an argon atmosphere, due to the retention of near stoichiometry maintaining sintering kinetics. SPS produced dense ceramics at similar sintering temperatures (1300C), but with greatly reduced sintering hold (5 minutes) and cycle times. However, microstructural inhomogeneity arose from the direct current polarity which led to oxygen ion diffusion toward the positive electrode. FS was performed with an alternating current electric field and produces samples of comparable density at sintering temperatures of ~1100C for a hold time of around 1 hour with no inhomogeneity due to the alternating current employed.

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citations
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
5
Average
Average
Top 10%
Green
hybrid