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Microstructure and defect analysis in the vicinity of blisters in polycrystalline tungsten

Microstructure and defect analysis in the vicinity of blisters in polycrystalline tungsten
Up to now, analyzing the production of dislocation-type defects in the subsurface region of plasma or ion-exposed tungsten samples has been hampered by the challenging production of suitable cross-section samples for transmission electron microscopy. We present two reliable methods based on precision electropolishing to prepare cross-sections of tungsten that allow direct imaging of dislocation-type defects by scanning as well as by transmission electron microscopy. Using these methods, we are able to demonstrate a clear enhancement of the dislocation density in the caps of blisters on tungsten exposed to H isotope plasma, i.e., of surface morphologies that are correlated to subsurface cavities. As a benchmark, we also show a cross-section of tungsten irradiated by 20 MeV W6+ ions.
Cross-section, TK9001-9401, Dislocations, Tungsten, Blistering; Cross-section; Dislocations; Electropolishing; Plasma; Tungsten, Plasma, Blistering, Electropolishing, Nuclear engineering. Atomic power
Cross-section, TK9001-9401, Dislocations, Tungsten, Blistering; Cross-section; Dislocations; Electropolishing; Plasma; Tungsten, Plasma, Blistering, Electropolishing, Nuclear engineering. Atomic power
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