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Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

descriptionPublicationkeyboard_double_arrow_right Article , Journal 01 Dec 2018 Spain, Sweden, France, Italy Publisher:Elsevier BVJournal:Nuclear Materials and Energy, volume 17, pages 295-301 (issn: 2352-1791, Copyright policy )Funded by:EC | EUROfusion
Authors: Kumar, M.; Makepeace, C.; Pardanaud, C.; Ferro, Y.; Hodille, E.; Martin, C.; Roubin, P.; +11 Authors

doi: 10.1016/j.nme.2018.11.008

handle: 11583/2986749

Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

Abstract

Beryllium oxide (BeO) and deuteroxide (BeOxDy) have been found on the melted zone of a beryllium tile extracted from the upper dump plate of JET-ILW (2011-2012 campaign). Results have been obtained using Raman microscopy, which is sensitive to both the chemical bond and crystal structure, with a micrometric lateral resolution. BeO is found with a wurtzite crystal structure. BeOxDy is found as three different types which are not the beta-phase but behaves as molecular species like Be(OD)(2), O(Be-D)(2) and DBeOD. The presence of a small amount of trapped D2O is also suspected. Our results therefore strongly suggest that D trapping occurs after melting through the formation of deuteroxides. The temperature increase favors the formation of crystal BeO which favors deuterium trapping through OD bonding. EURATOM 633053

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Keywords

[CHIM.MATE] Chemical Sciences/Material chemistry, Beryllium deuteroxide, TK9001-9401, [CHIM.MATE]Chemical Sciences/Material chemistry, Melting, Fusion, Plasma and Space Physics, [PHYS.PHYS.PHYS-CHEM-PH] Physics [physics]/Physics [physics]/Chemical Physics [physics.chem-ph], Fusion, plasma och rymdfysik, Beryllium oxide, Beryllium oxide; Beryllium deuteroxide; D trapping; Melting, Nuclear engineering. Atomic power, [PHYS.PHYS.PHYS-CHEM-PH]Physics [physics]/Physics [physics]/Chemical Physics [physics.chem-ph], D trapping

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citations
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
21
Top 10%
Top 10%
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