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Continuous salt precipitation and separation from supercritical water. Part 1: Type 1 salts

descriptionPublicationkeyboard_double_arrow_right Article , Journal 01 Feb 2010Publisher:Elsevier BVJournal:The Journal of Supercritical Fluids, volume 52, pages 99-112 (issn: 0896-8446,

Authors: Frédéric Vogel; M. Schubert; Johann W. Regler;

doi: 10.1016/j.supflu.2009.10.002

Continuous salt precipitation and separation from supercritical water. Part 1: Type 1 salts

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Abstract

Abstract The precipitation and separation performance of various binary type 1 salt–water mixtures was systematically studied for the first time in a continuously operated laboratory plant. The aim was to find a field of operation for the salt separator where salts can be separated with high efficiency. Experiments with aqueous solutions of the salts NaNO3, KNO3, Ca(NO3)2, K2CO3, KHCO3, (NH4)2CO3, K3PO4, K2HPO4, KH2PO4, NaCl, KCl, NH4Cl and (NH4)2SO4 were carried out at 30 ± 0.5 MPa varying the salt separator temperature from sub-critical to supercritical. For most of these salts separation efficiencies ranging from 80 to 97% were obtained. For the nitrates the separation efficiency increased in the order NaNO3

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Paul Scherrer Institute
Switzerland

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