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Development of High Power X-Ray Generator with LaB6Cathode and its Application to Fluorescence XAFS Measurement

Authors: K. Sakurai; N. Osaka;

Development of High Power X-Ray Generator with LaB6Cathode and its Application to Fluorescence XAFS Measurement

Abstract

The NRLM super XAFS is a high-power X-ray generator equipped with a compact rotating anode and a lanthanum hexaboride (LaB 6 ) cathode, specially developed for XAFS experiments. The design is different from the conventional source for X-ray diffraction, and the electron gun has enabled an extremely high tube-current (∼1,100 mA) even at low tube-voltage (14.5 ∼ 19.0 kV) when the beam is focused (around 0.07 mm at 6 deg. take off). The generator has an excellent stability and the filament life has been significantly prolonged by the unusual high vacuum specification of the tube. When a Johansson-type spectrometer is combined, intense monochromatic X-rays (5 x 10 6 - 10 7 counts/(sec.mm 2 ) at the sample position), which are completely free from higher order harmonics and tungsten contamination lines, are available. The present system has been applied to the fluorescence XAFS measurement, and it has been found that the spectrum with good quality can be obtained for thin films within 0.3 ∼ 1 day, and as for a transmission technique, the measuring time is quite short, 30 min ∼ 2 h.

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citations
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
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Average
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