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Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

Name: Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples
Keywords: melting, hydrogen, beryllium oxide, d trapping, beryllium deuteroxide, migration

descriptionPublicationkeyboard_double_arrow_right Article Switzerland

Authors: Kumar, M.; Makepeace, C.; Pardanaud, C.; Ferro, Y.; Hodille, E.; Martin, C.; Roubin, P.; +193 Authors

Kumar, M.; Makepeace, C.; Pardanaud, C.; Ferro, Y.; Hodille, E.; Martin, C.; Roubin, P.; Widdowson, A.; Dittmar, T.; Linsmeier, C. H.; Lungu, C. P.; Porosnicu, C.; Jepu, I; Dinca, P.; Lungu, M.; Pompilian, O. G.; Abduallev, S.; Abhangi, M.; Abreu, P.; Afzal, M.; Aggarwal, K. M.; Ahlgren, T.; Ahn, J. H.; Aho-Mantila, L.; Aiba, N.; Airila, M.; Albanese, R.; Aldred, V.; Alegre, D.; Alessi, E.; Aleynikov, P.; Alfier, A.; Alkseev, A.; Allinson, M.; Alper, B.; Alves, E.; Ambrosino, G.; Ambrosino, R.; Amicucci, L.; Amosov, V.; Sunden, E. Andersson; Angelone, M.; Anghel, M.; Angioni, C.; Appel, L.; Appelbee, C.; Arena, P.; Ariola, M.; Arnichand, H.; Arshad, S.; Ash, A.; Ashikawa, N.; Aslanyan, V.; Asunta, O.; Auriemma, F.; Austin, Y.; Avotina, L.; Axton, M. D.; Ayres, C.; Bacharis, M.; Baciero, A.; Baiao, D.; Bailey, S.; Baker, A.; Balboa, I.; Balden, M.; Balshaw, N.; Bament, R.; Banks, J. W.; Baranov, Y. F.; Barnard, M. A.; Barnes, D.; Barnes, M.; Barnsley, R.; Wiechec, A. Baron; Orte, L. Barrera; Baruzzo, M.; Basiuk, V.; Bassan, M.; Bastow, R.; Batista, A.; Batistoni, P.; Baughan, R.; Bauvir, B.; Baylor, L.; Bazylev, B.; Beal, J.; Beaumont, P. S.; Beckers, M.; Beckett, B.; Becoulet, A.; Bekris, N.; Beldishevski, M.; Bell, K.; Belli, F.; Bellinger, M.; Belonohy, E.; Ben Ayed, N.; Benterman, N. A.; Bergsaker, H.; Bernardo, J.; Bernert, M.; Berry, M.; Bertalot, L.; Besliu, C.; Beurskens, M.; Bieg, B.; Bielecki, J.; Biewer, T.; Bigi, M.; Bilkova, P.; Binda, F.; Bisoffi, A.; Bizarro, J. P. S.; Bjorkas, C.; Blackburn, J.; Blackman, K.; Blackman, T. R.; Blanchard, P.; Blatchford, P.; Bobkov, V.; Boboc, A.; Bodnar, G.; Bogar, O.; Bolshakova, I.; Bolzonella, T.; Bonanomi, N.; Bonelli, F.; Boom, J.; Booth, J.; Borba, D.; Borodin, D.; Borodkina, I.; Botrugno, A.; Bottereau, C.; Boulting, P.; Bourdelle, C.; Bowden, M.; Bower, C.; Bowman, C.; Boyce, T.; Boyd, C.; Boyer, H. J.; Bradshaw, J. M. A.; Braic, V.; Bravanec, R.; Breizman, B.; Bremond, S.; Brennan, P. D.; Breton, S.; Brett, A.; Brezinsek, S.; Bright, M. D. J.; Brix, M.; Broeckx, W.; Brombin, M.; Broslawski, A.; Brown, D. P. D.; Brown, M.; Bruno, E.; Bucalossi, J.; Buch, J.; Buchanan, J.; Buckley, M. A.; Budny, R.; Bufferand, H.; Bulman, M.; Bulmer, N.; Bunting, P.; Buratti, P.; Burckhart, A.; Buscarino, A.; Busse, A.; Butler, N. K.; Bykov, I.; Byrne, J.; Cahyna, P.; Calabro, G.; Calvo, I.; Camenen, Y.; Camp, P.; Campling, D. C.; Cane, J.; Cannas, B.; Capel, A. J.; Card, P. J.; Cardinali, A.; Carman, P.; Carr, M.; Carralero, D.; Carraro, L.; Carvalho, B. B.; Carvalho, I.; Carvalho, P.; Casson, F. J.; Castaldo, C.; Catarino, N.; Caumont, J.; Causa, F.; Cavazzana, R.;

Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

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Abstract

Beryllium oxide (BeO) and deuteroxide (BeOxDy) have been found on the melted zone of a beryllium tile extracted from the upper dump plate of JET-ILW (2011-2012 campaign). Results have been obtained using Raman microscopy, which is sensitive to both the chemical bond and crystal structure, with a micrometric lateral resolution. BeO is found with a wurtzite crystal structure. BeOxDy is found as three different types which are not the beta-phase but behaves as molecular species like Be(OD)(2), O(Be-D)(2) and DBeOD. The presence of a small amount of trapped D2O is also suspected. Our results therefore strongly suggest that D trapping occurs after melting through the formation of deuteroxides. The temperature increase favors the formation of crystal BeO which favors deuterium trapping through OD bonding.

Country

Switzerland

Related Organizations

École Polytechnique Fédérale de Lausanne EPFL
Switzerland

Keywords

melting, hydrogen, beryllium oxide, d trapping, beryllium deuteroxide, migration

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Found an issue? Give us feedback

Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

3 Research products, page 1 of 1

DEUTERATION OF FLUORENE AT C9 AND THE ASSIGNMENT OF CERTAIN BANDS IN THE INFRARED SPECTRUM TO THE AND GROUPS

Identification of BeO and BeOxDy in melted zones of the JET Be limiter tiles: Raman study using comparison with laboratory samples

The Infrared Absorption Spectra of Deuteroxide Solutions in Deuterium Oxide

DEUTERATION OF FLUORENE AT C₉ AND THE ASSIGNMENT OF CERTAIN BANDS IN THE INFRARED SPECTRUM TO THE AND GROUPS